N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine

Base Information

• Chemical Name: N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine
• CAS No.: 1226851-43-9
• Molecular Formula: C₂₈H₃₇N₃O
• Molecular Weight: 431.621

Synonyms:N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine

Chemical Property of N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine

Chemical Property:

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Technology Process of N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine

There total 5 articles about N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-benzyl-N-{2-[benzyl(N,N-dimethylglycyl)amino]ethyl}-3-methoxybenzamide → N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine (1226851-43-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 20h; Inert atmosphere; Reflux;

DOI:10.1016/j.ejmech.2016.03.045

Reference yield:

m-anisoyl chloride (1711-05-3) → N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine (1226851-43-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C / Inert atmosphere

2: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / chloroform / 0.25 h / 100 °C / Microwave irradiation

3: lithium aluminium tetrahydride / tetrahydrofuran / 20 h / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; dichloromethane; chloroform;

DOI:10.1016/j.ejmech.2016.03.045

Reference yield:

N,N'-Dibenzylethylenediamine (140-28-3,87170-83-0) → N,N'-dibenzyl-N-[2-(dimethylamino)ethyl]-N'-(3-methoxybenzyl)ethane-1,2-diamine (1226851-43-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 °C / Inert atmosphere

2: hydrogenchloride; water / tetrahydrofuran / 0.33 h / 120 °C / Microwave irradiation

3: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / chloroform / 0.25 h / 100 °C / Microwave irradiation

4: lithium aluminium tetrahydride / tetrahydrofuran / 20 h / Inert atmosphere; Reflux

With hydrogenchloride; lithium aluminium tetrahydride; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; dichloromethane; chloroform;

DOI:10.1016/j.ejmech.2016.03.045

upstream raw materials:

N,N'-Dibenzylethylenediamine

m-anisoyl chloride

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