diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate)

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Chemical Name:diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate)
CAS No.:1609250-21-6
Molecular Formula:C₄₀H₃₈O₁₀
Molecular Weight:678.736
Hs Code.:

Synonyms:diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate)

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Chemical Property of diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate)

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Technology Process of diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate)

There total 1 articles about diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 624-38-4,1032416-46-8
para-diiodobenzene

: 1465900-92-8
ethyl 5,6-dimethoxy-1-oxo-2-(prop-2-ynyl)-2,3-dihydro-1H-indene-2-carboxylate

: 1609250-18-1
ethyl 2-(3-(4-iodophenyl) prop-2-ynyl)-5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

: 1609250-21-6
diethyl 2,2'-(3,3'-(1,4-phenylene)bis(prop-2-yne-3,1-diyl))bis(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate)

Guidance literature:: para-diiodobenzene; With copper(l) iodide; palladium 10% on activated carbon; triethylamine; triphenylphosphine; In ethanol; for 0.5h; Inert atmosphere;

ethyl 5,6-dimethoxy-1-oxo-2-(prop-2-ynyl)-2,3-dihydro-1H-indene-2-carboxylate; In ethanol; for 2h; Reflux; Inert atmosphere;
DOI:10.1080/00397911.2013.860554