C₂₇H₃₂O₄N₂

Base Information

• Chemical Name: C₂₇H₃₂O₄N₂
• CAS No.: 247124-06-7
• Molecular Formula: C₂₇H₃₂N₂O₄
• Molecular Weight: 448.562
• Mol file: 247124-06-7.mol

Synonyms:C₂₇H₃₂O₄N₂

Chemical Property of C₂₇H₃₂O₄N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₂O₄N₂

There total 8 articles about C₂₇H₃₂O₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H32O5 (247123-98-4) → C27H32O4N2 (247124-06-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 2-methyl-2-butene; sodium chlorite; NaH₂PO₄ / 2-methyl-propan-2-ol; H₂O / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol;

DOI:10.1021/ol9902374

Reference yield:

C27H36O6 (247123-97-3) → C27H32O4N2 (247124-06-7)

Guidance literature:

Multi-step reaction with 3 steps

1: NaHCO₃; Pb(OAc)4 / CH₂Cl₂ / 0.83 h

2: 2-methyl-2-butene; sodium chlorite; NaH₂PO₄ / 2-methyl-propan-2-ol; H₂O / 20 °C

With lead(IV) acetate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydrogencarbonate; In dichloromethane; water; tert-butyl alcohol;

DOI:10.1021/ol9902374

Reference yield:

C28H42O3Si2 → C27H32O4N2 (247124-06-7)

Guidance literature:

Multi-step reaction with 6 steps

1: 10.8 g / TMSOTf; activated molecular sieves 4 Angstroem / CH₂Cl₂; tetrahydrofuran / 1 h / 0 °C

2: 5.0 g / TBAF; AcOH / tetrahydrofuran / 2 h / 20 °C

3: tetrahydrofuran; diethyl ether / 1 h / -78 - -20 °C

4: NaHCO₃; Pb(OAc)4 / CH₂Cl₂ / 0.83 h

5: 2-methyl-2-butene; sodium chlorite; NaH₂PO₄ / 2-methyl-propan-2-ol; H₂O / 20 °C

With lead(IV) acetate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;

DOI:10.1021/ol9902374

upstream raw materials:

C₂₆H₃₂O₆

potassium cyanide

C₂₇H₃₆O₆

C₂₆H₃₂O₅

Downstream raw materials:

C₂₇H₃₂O₃SN₂