Technology Process of C25H22N2O5S
There total 9 articles about C25H22N2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H26N2O5S;
With
lithium hydroxide monohydrate;
In
methanol;
at 20 ℃;
With
hydrogenchloride;
In
methanol; water;
pH=3 - 4;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,4-dioxane / Reflux; Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
3.1: pyridine / 50 °C
4.1: lithium hydroxide monohydrate / methanol / 20 °C
4.2: pH 3 - 4
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium hydroxide monohydrate; sodium carbonate; trifluoroacetic acid;
In
1,4-dioxane; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 90 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,4-dioxane / Reflux; Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
4.1: pyridine / 50 °C
5.1: lithium hydroxide monohydrate / methanol / 20 °C
5.2: pH 3 - 4
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; lithium hydroxide monohydrate; diphenyl phosphoryl azide; sodium carbonate; triethylamine; trifluoroacetic acid;
In
1,4-dioxane; methanol; dichloromethane; water; toluene;