N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

Base Information

Chemical Name:N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide
CAS No.:1613039-79-4
Molecular Formula:C₁₈H₁₃F₁₃N₄O
Molecular Weight:548.307
Hs Code.:

Synonyms:N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

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Chemical Property of N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

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Technology Process of N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

There total 3 articles about N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazole-4-carbaldehyde

: 29601-98-7
N-benzylhydroxylamine hydrochloride

: 1613039-79-4
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

Guidance literature:: With sodium hydrogencarbonate; In ethanol; at 60 ℃;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 929200-08-8
(1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methanol

: 1613039-79-4
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: Jones reagent / acetone / 0.58 h / 0 °C

2: sodium hydrogencarbonate / ethanol / 60 °C

With Jones reagent; sodium hydrogencarbonate; In ethanol; acetone;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 62571-55-5
8-azido-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane

: 1613039-79-4
N-((1-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-1H-1,2,3-triazol-4-yl)methylene)-1-phenylmethanamine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: copper diacetate / water; tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere

2: Jones reagent / acetone / 0.58 h / 0 °C

3: sodium hydrogencarbonate / ethanol / 60 °C

With Jones reagent; copper diacetate; sodium hydrogencarbonate; In ethanol; water; acetone; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2014.04.052