ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

Base Information

Chemical Name:ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate
CAS No.:1393449-03-0
Molecular Formula:C₂₇H₃₇NO₃
Molecular Weight:423.596
Hs Code.:

Synonyms:ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

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Chemical Property of ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

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Technology Process of ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

There total 2 articles about ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1393449-04-1
trans-4-ethylcyclohexyl methanesulfonate

: 1393448-85-5
ethyl 1-((6-hydroxynaphthalen-2-yl)methyl)piperidine-4-carboxylate

: 1393449-03-0
ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

Guidance literature:: ethyl 1-((6-hydroxynaphthalen-2-yl)methyl)piperidine-4-carboxylate; With caesium carbonate; In butanone; tert-butyl alcohol; at 80 ℃; for 0.166667h;

trans-4-ethylcyclohexyl methanesulfonate; In butanone; tert-butyl alcohol; at 80 ℃; for 15h; Inert atmosphere;

Reference yield:

: 78119-82-1
6-hydroxynaphthalene-2-carbaldehyde

: 1393449-03-0
ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid; sodium tris(acetoxy)borohydride / 2 h / 20 °C

2.1: caesium carbonate / butanone; tert-butyl alcohol / 0.17 h / 80 °C

2.2: 15 h / 80 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; caesium carbonate; toluene-4-sulfonic acid; In butanone; tert-butyl alcohol;

Reference yield: 71.0%

: 1393449-03-0
ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate

: 1393449-05-2
1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylic acid

Guidance literature:: ethyl 1-((6-(cis-4-ethylcyclohexyloxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate; With water; sodium hydroxide; In ethanol; for 2h; Reflux;

With hydrogenchloride; In water; pH=7;