1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI)

Base Information

Chemical Name:1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI)
CAS No.:288088-59-5
Molecular Formula:C₆H₁₃NO₄
Molecular Weight:163.174
Hs Code.:
Mol file:288088-59-5.mol

Synonyms:1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI)

Suppliers and Price of 1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI)

Chemical Property:

PSA：95.94000
LogP:-1.87470

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI)

There total 12 articles about 1,2,3-Cyclopentanetriol,4-amino-5-methoxy-,(1R,2R,3R,4S,5R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 288088-79-9
1L-(1,2,3,4,5/0)-1,2,3-tri-O-acetyl-5-acetamido-4-O-methyl-1,2,3,4-cyclopentanetetrol

: 288088-59-5,288088-61-9
(1S,2R,3R,4R,5S)-5-amino-1-O-methyl-1,2,3,4-cyclopentanetetrol

Guidance literature:: With barium dihydroxide; at 90 ℃;
DOI:10.1002/ejoc.200500118

Reference yield: 42.0%

: 288088-78-8
1L-(1,2,3,5/4)-1,2,3-tri-O-acetyl-5-acetamido-4-O-methyl-1,2,3,4-cyclopentanetetrol

: 288088-59-5,288088-61-9
(1R,2R,3R,4R,5S)-5-amino-4-O-methyl-1,2,3,4-cyclopentanetetrol

Guidance literature:: With barium dihydroxide; at 90 ℃; for 5h;
DOI:10.1002/ejoc.200500118

Reference yield:

: 171031-90-6
C₂₃H₂₉NO₈

: 288088-59-5,288088-61-9
(1S,2R,3R,4R,5S)-5-amino-1-O-methyl-1,2,3,4-cyclopentanetetrol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 °C

2.1: 66 mg / sodium methoxide / methanol; CH₂Cl₂ / 0.5 h / 0 °C

3.1: 97 percent / silver oxide / acetonitrile / 80 °C

4.1: H₂O; acetic acid / 9 h / 80 °C

4.2: 87 percent / pyridine / 20 °C

5.1: 100 percent / 1 M aq. barium hydroxide / 90 °C

With 2,6-dimethylpyridine; barium dihydroxide; sodium methylate; silver(l) oxide; In methanol; dichloromethane; water; acetic acid; acetonitrile; 2.1: Zemplen deacylation;
DOI:10.1002/ejoc.200500118