3-benzyl-8-methyl-3a,4,5,6-tetrahydro-1H-pyrazino[3,2,1-jk]carbazol-2(3H)-one

Base Information

Chemical Name:3-benzyl-8-methyl-3a,4,5,6-tetrahydro-1H-pyrazino[3,2,1-jk]carbazol-2(3H)-one
CAS No.:115174-31-7
Molecular Formula:C₂₂H₂₂N₂O
Molecular Weight:330.429
Hs Code.:
Mol file:115174-31-7.mol

Synonyms:3-benzyl-6-methyl-2-oxo-2,3,3a,4,5,6-hexahydro-1H-pyrazine<3,2,1-j,k>carbazole

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Chemical Property of 3-benzyl-8-methyl-3a,4,5,6-tetrahydro-1H-pyrazino[3,2,1-jk]carbazol-2(3H)-one

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Technology Process of 3-benzyl-8-methyl-3a,4,5,6-tetrahydro-1H-pyrazino[3,2,1-jk]carbazol-2(3H)-one

There total 7 articles about 3-benzyl-8-methyl-3a,4,5,6-tetrahydro-1H-pyrazino[3,2,1-jk]carbazol-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 115174-33-9
1-benzylamino-6-methyl-9-carbomethoxymethyl-1,2,3,4-tetrahydrocarbazole

: 115174-31-7
3-benzyl-6-methyl-2-oxo-2,3,3a,4,5,6-hexahydro-1H-pyrazine<3,2,1-j,k>carbazole

Guidance literature:: In xylene; for 5h; Heating;
DOI:10.1007/BF00472254

Reference yield: 52.0%

: 115174-35-1
N-benzyl-N-(6-methyl-1,2,3,4-tetrahydro-1-carbazolyl)chloroacetamide

: 115174-31-7
3-benzyl-6-methyl-2-oxo-2,3,3a,4,5,6-hexahydro-1H-pyrazine<3,2,1-j,k>carbazole

Guidance literature:: With sodium hydroxide; In benzene; at 65 ℃; for 0.5h; phase transfer with tetrabutylammonium bromide;
DOI:10.1007/BF00472254

Reference yield:

: 3449-48-7,812649-03-9
6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 115174-31-7
3-benzyl-6-methyl-2-oxo-2,3,3a,4,5,6-hexahydro-1H-pyrazine<3,2,1-j,k>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / xylene / 3 h / Heating

2: NaBH₄ / ethanol / 4 h / 20 °C

3: triethylamine / toluene / 2 h / 20 °C

4: 52 percent / 50percent NaOH / benzene / 0.5 h / 65 °C / phase transfer with tetrabutylammonium bromide

With sodium hydroxide; sodium tetrahydroborate; triethylamine; In ethanol; toluene; xylene; benzene;
DOI:10.1007/BF00472254