4-methyl-3-oxo-1,2-diazetidinium tosylate

Base Information

Chemical Name:4-methyl-3-oxo-1,2-diazetidinium tosylate
CAS No.:79289-51-3
Molecular Formula:C₃H₆N₂O*C₇H₈O₃S
Molecular Weight:258.298
Hs Code.:

Synonyms:4-methyl-3-oxo-1,2-diazetidinium tosylate

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Chemical Property of 4-methyl-3-oxo-1,2-diazetidinium tosylate

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Technology Process of 4-methyl-3-oxo-1,2-diazetidinium tosylate

There total 1 articles about 4-methyl-3-oxo-1,2-diazetidinium tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 79289-32-0
1-(diphenylmethylene)-4-methyl-3-oxo-1,2-diazetidinium hydroxide, inner salt

: 104-15-4
toluene-4-sulfonic acid

: 79289-51-3
4-methyl-3-oxo-1,2-diazetidinium tosylate

Guidance literature:: In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/ja00416a009

Reference yield: 82.0%

: 79289-51-3
4-methyl-3-oxo-1,2-diazetidinium tosylate

: 122-57-6
1-Phenylbut-1-en-3-one

: 92184-57-1
(E)-1-(4-phenyl-2-but-3-enylidene)-4-methyl-3-oxo-1,2-diazetidinium inner salt

Guidance literature:: In N,N-dimethyl-formamide; at 0 ℃; for 1.5h;
DOI:10.1021/jo00197a017

Reference yield:

: 79289-51-3
4-methyl-3-oxo-1,2-diazetidinium tosylate

: 92184-64-0
1-(3-methyl-1-phenyl-3-but-1-enyl)-4-methyl-1,2-diazetidin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / dimethylformamide / 1.5 h / 0 °C

2: 81 percent / tetrahydrofuran / 0 °C

In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00197a017