C₁₆H₁₄F₃NO₄S

Base Information

Chemical Name:C₁₆H₁₄F₃NO₄S
CAS No.:1380243-47-9
Molecular Formula:C₁₆H₁₄F₃NO₄S
Molecular Weight:373.353
Hs Code.:

C<sub>16</sub>H<sub>14</sub>F<sub>3</sub>NO<sub>4</sub>S

Synonyms:C₁₆H₁₄F₃NO₄S

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Chemical Property of C₁₆H₁₄F₃NO₄S

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Technology Process of C₁₆H₁₄F₃NO₄S

There total 8 articles about C₁₆H₁₄F₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1380243-44-6
C₁₆H₁₆F₃NO₃S

: 1380243-47-9
C₁₆H₁₄F₃NO₄S

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 1380243-33-3
C₁₇H₁₈F₃NO₂S₂

: 1380243-47-9
C₁₆H₁₄F₃NO₄S

Guidance literature:: Multi-step reaction with 2 steps

1: methyl iodide; water / methanol / 0.5 h / 20 °C / Cooling with ice

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; sodium bromide; sodium hydrogencarbonate / dichloromethane / 2 h / 0 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; water; sodium hydrogencarbonate; sodium bromide; methyl iodide; In methanol; dichloromethane;

Reference yield:

: 327-52-6
1-bromo-2,4,5-trifluorobenzene

: 1380243-47-9
C₁₆H₁₄F₃NO₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert-butylmagnesium bromide; copper(I) bromide dimethylsulfide complex / tetrahydrofuran / 0.25 h / -20 - -5 °C / Inert atmosphere

1.2: 0.08 h

2.1: methyl iodide; water / methanol / 0.5 h / 20 °C / Cooling with ice

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; sodium bromide; sodium hydrogencarbonate / dichloromethane / 2 h / 0 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; copper(I) bromide dimethylsulfide complex; tert-butylmagnesium bromide; water; sodium hydrogencarbonate; sodium bromide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane;