C₁₄H₁₆FN₃S

Base Information

Chemical Name:C₁₄H₁₆FN₃S
CAS No.:1310839-80-5
Molecular Formula:C₁₄H₁₆FN₃S
Molecular Weight:277.366
Hs Code.:

C<sub>14</sub>H<sub>16</sub>FN<sub>3</sub>S

Synonyms:C₁₄H₁₆FN₃S

Suppliers and Price of C₁₄H₁₆FN₃S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₆FN₃S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₆FN₃S

There total 13 articles about C₁₄H₁₆FN₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310839-78-1
C₂₀H₁₉FN₄O₄S₂

: 1310839-80-5
C₁₄H₁₆FN₃S

Guidance literature:: With triethylamine; p-Chlorothiophenol; In ISOPROPYLAMIDE; at 20 - 60 ℃; for 2h;

Reference yield:

: 4117-10-6
6-hepten-1-ol

: 1310839-80-5
C₁₄H₁₆FN₃S

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 20 °C / Reflux

1.2: 1.5 h / 20 °C

2.1: sodium hypochlorite / dichloromethane; water / 0.5 h / 20 °C

3.1: n-butyllithium / toluene; hexane; tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere

3.2: 0.42 h / -70 °C / Inert atmosphere

3.3: 1.25 h / -70 °C / Inert atmosphere

4.1: nitric acid; sulfuric acid / 1 h / Cooling with ice

5.1: ammonium chloride; iron / ethanol; water / 2 h / 20 - 45 °C

6.1: triethylamine / methanol / 4 h / 20 °C

7.1: hydrogen / 5% rhodium-on-charcoal / ethanol / 23 h / 20 °C

8.1: tetrahydrofuran / 14 h / 20 - 70 °C

9.1: potassium carbonate / water; tetrahydrofuran; methanol / 5.5 h / 20 - 50 °C

10.1: triethylamine / water; tetrahydrofuran / 4.5 h / 20 °C / Cooling with ice

11.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / 20 °C / Reflux

11.2: 2 h / 20 °C

12.1: acetone / 0.83 h / 20 °C / Cooling with ice

13.1: sulfuric acid / 15.5 h / 20 °C

14.1: triethylamine; p-Chlorothiophenol / ISOPROPYLAMIDE / 2 h / 20 - 60 °C

With sodium hypochlorite; n-butyllithium; sulfuric acid; hydrogen; nitric acid; iron; potassium carbonate; ammonium chloride; triethylamine; p-Chlorothiophenol; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; ISOPROPYLAMIDE; water; ethyl acetate; acetone; toluene;

Reference yield:

: 3,3a,4,5,6,7-hexahydrobenzo[c]isoxazole

: 1310839-80-5
C₁₄H₁₆FN₃S

Guidance literature:: Multi-step reaction with 12 steps

1.1: n-butyllithium / toluene; hexane; tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere

1.2: 0.42 h / -70 °C / Inert atmosphere

1.3: 1.25 h / -70 °C / Inert atmosphere

2.1: nitric acid; sulfuric acid / 1 h / Cooling with ice

3.1: ammonium chloride; iron / ethanol; water / 2 h / 20 - 45 °C

4.1: triethylamine / methanol / 4 h / 20 °C

5.1: hydrogen / 5% rhodium-on-charcoal / ethanol / 23 h / 20 °C

6.1: tetrahydrofuran / 14 h / 20 - 70 °C

7.1: potassium carbonate / water; tetrahydrofuran; methanol / 5.5 h / 20 - 50 °C

8.1: triethylamine / water; tetrahydrofuran / 4.5 h / 20 °C / Cooling with ice

9.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 6 h / 20 °C / Reflux

9.2: 2 h / 20 °C

10.1: acetone / 0.83 h / 20 °C / Cooling with ice

11.1: sulfuric acid / 15.5 h / 20 °C

12.1: triethylamine; p-Chlorothiophenol / ISOPROPYLAMIDE / 2 h / 20 - 60 °C

With n-butyllithium; sulfuric acid; hydrogen; nitric acid; iron; potassium carbonate; ammonium chloride; triethylamine; p-Chlorothiophenol; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; 5% rhodium-on-charcoal; In tetrahydrofuran; methanol; ethanol; hexane; ISOPROPYLAMIDE; water; ethyl acetate; acetone; toluene;