10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane

Base Information

Chemical Name:10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane
CAS No.:871822-73-0
Molecular Formula:C₃₉H₃₉BN₂O₂
Molecular Weight:578.562
Hs Code.:

Synonyms:10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane

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Chemical Property of 10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane

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Technology Process of 10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane

There total 2 articles about 10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 74032-45-4
S-2-pyridyl 4-methylbenzothiolate

: 871822-73-0
10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane

Guidance literature:: 10-(9-borabicyclo[3.3.1]non-9-yl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane; With ethylmagnesium bromide; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; at 0 - 20 ℃; for 0.166667 - 0.25h;

S-2-pyridyl 4-methylbenzothiolate; In tetrahydrofuran; at 20 ℃; for 0.5h;

With water; ammonium chloride; In tetrahydrofuran; Product distribution / selectivity;

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 871822-73-0
10-(9-borabicyclo[3.3.1]non-9-yl)-5-phenyl-1,9-di-p-toluoyldipyrromethane

Guidance literature:: 10-(9-borabicyclo[3.3.1]non-9-yl)-1-(4-methylbenzoyl)-5-phenyldipyrromethane; With 2,2,6,6-tetramethyl-piperidine; ethylmagnesium bromide; In tetrahydrofuran; at 0 - 20 ℃;

4-methyl-benzoyl chloride; In tetrahydrofuran; Product distribution / selectivity;