C₁₂H₁₁BrFNO₃S

Base Information

Chemical Name:C₁₂H₁₁BrFNO₃S
CAS No.:1300699-40-4
Molecular Formula:C₁₂H₁₁BrFNO₃S
Molecular Weight:348.193
Hs Code.:

C<sub>12</sub>H<sub>11</sub>BrFNO<sub>3</sub>S

Synonyms:C₁₂H₁₁BrFNO₃S

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Chemical Property of C₁₂H₁₁BrFNO₃S

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Technology Process of C₁₂H₁₁BrFNO₃S

There total 5 articles about C₁₂H₁₁BrFNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1300699-39-1
C₁₂H₁₂FNO₄S

: 1300699-40-4
C₁₂H₁₁BrFNO₃S

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 854015-42-2
ethyl 5-bromo-4-methyl-1,2-oxazole-3-carboxylate

: 1300699-40-4
C₁₂H₁₁BrFNO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; methanol / tetrahydrofuran / -20 - 20 °C

1.2: 10 °C / pH 4 - 5

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 15 h / 110 °C / Sealed tube

3.1: triphenylphosphine; N-Bromosuccinimide / dichloromethane / 0 - 20 °C

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; potassium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;

Reference yield:

: 759-65-9
diethyl oxalpropionate

: 1300699-40-4
C₁₂H₁₁BrFNO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydroxylamine hydrochloride / ethanol / 12 h / Reflux

2.1: triethylamine; phosphorus(V) oxybromide / -20 - 80 °C

3.1: sodium tetrahydroborate; methanol / tetrahydrofuran / -20 - 20 °C

3.2: 10 °C / pH 4 - 5

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 15 h / 110 °C / Sealed tube

5.1: triphenylphosphine; N-Bromosuccinimide / dichloromethane / 0 - 20 °C

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; hydroxylamine hydrochloride; potassium carbonate; triethylamine; triphenylphosphine; phosphorus(V) oxybromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;