C₂₃H₂₄ClNO₃

Base Information

Chemical Name:C₂₃H₂₄ClNO₃
CAS No.:1253214-96-8
Molecular Formula:C₂₃H₂₄ClNO₃
Molecular Weight:397.901
Hs Code.:

C<sub>23</sub>H<sub>24</sub>ClNO<sub>3</sub>

Synonyms:C₂₃H₂₄ClNO₃

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Chemical Property of C₂₃H₂₄ClNO₃

Chemical Property:

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Technology Process of C₂₃H₂₄ClNO₃

There total 6 articles about C₂₃H₂₄ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 939430-71-4
6-chloro-5-methoxymethoxy-pyridine-2-carbaldehyde

: 1253214-96-8
C₂₃H₂₄ClNO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: acetic acid / ethanol / 7 h / 50 °C

3.1: caesium carbonate / tetrahydrofuran; acetonitrile / 4 h

4.1: pyridine / 18 h

5.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C / Cooling with ice

With pyridine; triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; caesium carbonate; acetic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetonitrile;

Reference yield:

: 848442-41-1
C₁₂H₁₇BrO₂

: 1253214-96-8
C₂₃H₂₄ClNO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 2.83 h / -78 - 20 °C

2.1: acetic acid / ethanol / 7 h / 50 °C

3.1: caesium carbonate / tetrahydrofuran; acetonitrile / 4 h

4.1: pyridine / 18 h

5.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C / Cooling with ice

With pyridine; triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; caesium carbonate; acetic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetonitrile;

Reference yield:

: 1253214-82-2
C₂₀H₂₆ClNO₅

: 1253214-96-8
C₂₃H₂₄ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / ethanol / 7 h / 50 °C

2: caesium carbonate / tetrahydrofuran; acetonitrile / 4 h

3: pyridine / 18 h

4: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0.17 h / 0 °C / Cooling with ice

With pyridine; triethylsilane; boron trifluoride diethyl etherate; caesium carbonate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;