C₃₀H₄₄O₃Si

Base Information

Chemical Name:C₃₀H₄₄O₃Si
CAS No.:934808-36-3
Molecular Formula:C₃₀H₄₄O₃Si
Molecular Weight:480.763
Hs Code.:

C<sub>30</sub>H<sub>44</sub>O<sub>3</sub>Si

Synonyms:C₃₀H₄₄O₃Si

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Chemical Property of C₃₀H₄₄O₃Si

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Technology Process of C₃₀H₄₄O₃Si

There total 1 articles about C₃₀H₄₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 934558-86-8
C₂₆H₄₀O₂Si

: 2605-68-7
methyl 2-(triphenylphosphoranylidene)propionate

: 934808-36-3
C₃₀H₄₄O₃Si

Guidance literature:: C₂₆H₄₀O₂Si; With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroem MS; In dichloromethane; at 25 ℃; for 0.5h;

methyl 2-(triphenylphosphoranylidene)propionate; In toluene; at 80 ℃; for 12h; Further stages.;
DOI:10.1021/ol070298z

Reference yield: 80.0%

: 934808-36-3
C₃₀H₄₄O₃Si

: 934808-37-4
C₂₉H₄₆O₂Si

: C₂₉H₄₆O₂Si

Guidance literature:: C₃₀H₄₄O₃Si; With hydrogen; irridium catalyst; In dichloromethane; at 25 ℃; for 4h; under 38002.6 Torr;

With diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1021/ol070298z

Reference yield:

: 934808-36-3
C₃₀H₄₄O₃Si

: 934808-38-5
C₃₁H₅₀OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / irridium catalyst / CH₂Cl₂ / 4 h / 25 °C / 38002.6 Torr

1.2: 80 percent / DIBALH / tetrahydrofuran; CH₂Cl₂ / 0.5 h / 0 °C

2.1: NMO; TPAP; 4 Angstroem MS / CH₂Cl₂ / 0.5 h / 25 °C

2.2: tetrahydrofuran; toluene / 1 h / -78 °C

2.3: 76 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 7 h / 25 °C

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroem MS; hydrogen; irridium catalyst; In dichloromethane;
DOI:10.1021/ol070298z