N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

Base Information

Chemical Name:N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea
CAS No.:162414-07-5
Molecular Formula:C₄₂H₅₀N₂O₉S
Molecular Weight:758.933
Hs Code.:

Synonyms:N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

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Chemical Property of N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

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Technology Process of N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

There total 1 articles about N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

: 32780-32-8
validamine

: 93173-26-3
2,3,4,6-Tetra-O-benzyl-α-D-glucopyranosyl isothiocyanate

: 162414-07-5
N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

Guidance literature:: In water; N,N-dimethyl-formamide; for 0.666667h; Ambient temperature;

Reference yield: 94.8%

: 162414-07-5
N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

: 162414-08-6
(1S,3R,4R,5S,6S)-3-hydroxymethyl-8-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosylamino)-7-oxa-9-azabicyclo<4.3.0>non-8-ene-4,5-diol

Guidance literature:: With mercury(II) oxide; In diethyl ether; for 46h; Ambient temperature;

Reference yield:

: 162414-07-5
N-<(1S)-(1,2,4/3,5)-2,3,4-trihydroxy-5-(hydroxymethyl)cyclohexyl>-N'-(2',3',4',6'-tetra-O-benzyl-α-D-glucopyranosyl)thiourea

: 162414-09-7
(1S,5S,7R,8S,1''R)-3-(5a'-carba-α-D-glucopyranosylamino)-7-(1'',2''-dihydroxyethyl)-2,6-dioxa-4-azabicyclo<3.3.0>oct-3-en-8-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 94.8 percent / HgO / diethyl ether / 46 h / Ambient temperature

2: 85.7 percent / Na / liquid ammonia; tetrahydrofuran / 0.25 h / -78 °C

With sodium; mercury(II) oxide; In tetrahydrofuran; diethyl ether; ammonia;