C₅₀H₇₀O₇Si₂

Base Information

Chemical Name:C₅₀H₇₀O₇Si₂
CAS No.:164530-20-5
Molecular Formula:C₅₀H₇₀O₇Si₂
Molecular Weight:839.273
Hs Code.:

C<sub>50</sub>H<sub>70</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₅₀H₇₀O₇Si₂

Suppliers and Price of C₅₀H₇₀O₇Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₀H₇₀O₇Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₀H₇₀O₇Si₂

There total 16 articles about C₅₀H₇₀O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 164530-17-0
Acetic acid (2S,4aS,4bS,6R,6aR,6bR,9aS,10bR,12aS)-2-acetoxy-8-((R)-1-hydroxy-3-methyl-but-3-enyl)-4a,6a,7-trimethyl-6b-trimethylsilanyloxy-2,3,4,4a,4b,5,6,6a,6b,9a,10b,11,12,12a-tetradecahydro-1H-9-oxa-pentaleno[2,1-a]phenanthren-6-yl ester

: 164530-20-5
C₅₀H₇₀O₇Si₂

Guidance literature:: With silver nitrate; In N,N-dimethyl-formamide; for 0.25h;
DOI:10.1021/ja9817139

Reference yield:

: 5821-04-5
3β,12β-diacetoxy-5α-pregn-16-en-20-one

: 164530-20-5
C₅₀H₇₀O₇Si₂

Guidance literature:: Multi-step reaction with 14 steps

1: 1.) NBS, benzoyl peroxide, 2.) aq. NaOH, H₂O₂, 3.) Ac₂O, pyridine

2: 99 percent / Zn, CuI, H₂O / ethanol / 15 h / 25 °C / Irradiation

3: 94 percent / pyridine / 1 h / 0 °C

4: 96 percent / OsO₄, pyridine / 10 h / 25 °C

5: SOCl₂, pyridine / 0.5 h

6: NaIO₄, RuCl₃*H₂O / acetonitrile; H₂O / 0.17 h

7: 90 percent / toluene / 15 h / Heating

8: mCPBA / CH₂Cl₂ / 3 h

9: aq. H₂SO₄ / tetrahydrofuran / 2 h

10: Rh₂(OAc)2 / benzene / 6 h / Heating

11: NaH / tetrahydrofuran / 0.5 h

12: 1.) LiBH₄, 2.) MnO₂, 3.) Ac₂O, Et₃N, DMAP

13: 126 mg / lithium perchlorate diethyl ether / 1 h

14: 98 percent / AgNO₃ / dimethylformamide / 0.25 h

With pyridine; dmap; manganese(IV) oxide; ruthenium trichloride; dirhodium tetraacetate; sodium hydroxide; sodium periodate; N-Bromosuccinimide; copper(l) iodide; osmium(VIII) oxide; lithium borohydride; thionyl chloride; Perbenzoic acid; sulfuric acid; water; dihydrogen peroxide; lithium perchlorate; acetic anhydride; sodium hydride; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1021/ja9817139

Reference yield:

: 161254-90-6
Acetic acid (3S,5S,8R,9S,10S,12R,13R,14S,15S,16S,17S)-3-acetoxy-17-acetyl-15-bromo-10,13-dimethyl-hexadecahydro-20-oxa-cyclopropa[16,17]cyclopenta[a]phenanthren-12-yl ester

: 164530-20-5
C₅₀H₇₀O₇Si₂

Guidance literature:: Multi-step reaction with 13 steps

1: 99 percent / Zn, CuI, H₂O / ethanol / 15 h / 25 °C / Irradiation

2: 94 percent / pyridine / 1 h / 0 °C

3: 96 percent / OsO₄, pyridine / 10 h / 25 °C

4: SOCl₂, pyridine / 0.5 h

5: NaIO₄, RuCl₃*H₂O / acetonitrile; H₂O / 0.17 h

6: 90 percent / toluene / 15 h / Heating

7: mCPBA / CH₂Cl₂ / 3 h

8: aq. H₂SO₄ / tetrahydrofuran / 2 h

9: Rh₂(OAc)2 / benzene / 6 h / Heating

10: NaH / tetrahydrofuran / 0.5 h

11: 1.) LiBH₄, 2.) MnO₂, 3.) Ac₂O, Et₃N, DMAP

12: 126 mg / lithium perchlorate diethyl ether / 1 h

13: 98 percent / AgNO₃ / dimethylformamide / 0.25 h

With pyridine; dmap; manganese(IV) oxide; ruthenium trichloride; dirhodium tetraacetate; sodium periodate; copper(l) iodide; osmium(VIII) oxide; lithium borohydride; thionyl chloride; sulfuric acid; water; lithium perchlorate; acetic anhydride; sodium hydride; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1021/ja9817139