C₂₃H₃₀O₄

Base Information

Chemical Name:C₂₃H₃₀O₄
CAS No.:1612188-59-6
Molecular Formula:C₂₃H₃₀O₄
Molecular Weight:370.489
Hs Code.:

C<sub>23</sub>H<sub>30</sub>O<sub>4</sub>

Synonyms:C₂₃H₃₀O₄

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Chemical Property of C₂₃H₃₀O₄

Chemical Property:

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Technology Process of C₂₃H₃₀O₄

There total 9 articles about C₂₃H₃₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1612188-58-5
C₂₃H₃₄O₂

: 1612188-59-6
C₂₃H₃₀O₄

Guidance literature:: With sodium periodate; ruthenium(III) chloride trihydrate; In tetrachloromethane; acetonitrile; at 22 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja503972p

Reference yield:

: 1612188-54-1
7-epi-taiwaniaquinone F

: 1612188-59-6
C₂₃H₃₀O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: ozone; triphenylphosphine / dichloromethane / 4 h / -78 - 22 °C / Inert atmosphere

2.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 22 °C / Inert atmosphere

3.1: hydrazine hydrate / diethylene glycol / 2 h / 22 - 160 °C / Inert atmosphere

3.2: 4 h / 22 - 180 °C / Inert atmosphere

4.1: sodium periodate; ruthenium(III) chloride trihydrate / acetonitrile; tetrachloromethane / 2 h / 22 °C / Inert atmosphere

With sodium periodate; ruthenium(III) chloride trihydrate; potassium tert-butylate; ozone; hydrazine hydrate; triphenylphosphine; In tetrachloromethane; dichloromethane; acetonitrile; tert-butyl alcohol; diethylene glycol; 3.1: |Wolff-Kishner-Huang Minlon Reduction;
DOI:10.1021/ja503972p

Reference yield:

: 818-50-8
4-methyl-hexa-3,5-dien-1-ol

: 1612188-59-6
C₂₃H₃₀O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 22 °C / Inert atmosphere

2.1: bis-(1,2-dimethylpropyl)borane / 24 h / 0 - 22 °C / Inert atmosphere

2.2: 16 h / 22 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 22 °C / Inert atmosphere

4.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; zinc trifluoromethanesulfonate; (R)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine / 1,2-dichloro-ethane / 24 h / 22 °C / Inert atmosphere

4.2: 2.5 h / 0 - 22 °C / Inert atmosphere

5.1: ozone; triphenylphosphine / dichloromethane / 4 h / -78 - 22 °C / Inert atmosphere

6.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 22 °C / Inert atmosphere

7.1: hydrazine hydrate / diethylene glycol / 2 h / 22 - 160 °C / Inert atmosphere

7.2: 4 h / 22 - 180 °C / Inert atmosphere

8.1: sodium periodate; ruthenium(III) chloride trihydrate / acetonitrile; tetrachloromethane / 2 h / 22 °C / Inert atmosphere

With 1H-imidazole; sodium periodate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (R)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-5H-dibenz[b,f]azepine; ruthenium(III) chloride trihydrate; potassium tert-butylate; tetrabutyl ammonium fluoride; bis-(1,2-dimethylpropyl)borane; zinc trifluoromethanesulfonate; ozone; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; tetrachloromethane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; diethylene glycol; 7.1: |Wolff-Kishner-Huang Minlon Reduction;
DOI:10.1021/ja503972p