1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

Base Information

Chemical Name:1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A
CAS No.:129254-32-6
Molecular Formula:C₂₅H₂₇N₃O₈S
Molecular Weight:529.571
Hs Code.:

Synonyms:1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

Suppliers and Price of 1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

There total 2 articles about 1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 122644-75-1
6-Demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-methylidenemitosane

: 108-98-5
thiophenol

: 129254-32-6
1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

Guidance literature:: With triethylamine; In chloroform; for 1.5h; Ambient temperature;
DOI:10.1021/jm00038a008

Reference yield:

: 122644-74-0,122675-60-9,134679-23-5
1a-acetyl-7-demethoxy-6,7-dihydro-7,7-(ethylenedioxy)-6-(phenylselenyl)mitomycin A

: 129254-32-6
1a-acetyl-7-demethoxy-6-demethyl-7,7-(ethylenedioxy)-6,7-dihydro-6-<(phenythio)methyl>mitomycin A

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, mCPBA / CHCl₃ / 0.17 h / Ambient temperature

2: 71 percent / Et₃N / CHCl₃ / 1.5 h / Ambient temperature

With pyridine; triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1021/jm00038a008