3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate

Base Information

• Chemical Name: 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate
• CAS No.: 1584677-19-9
• Molecular Formula: C₁₈H₂₈O₆S₂
• Molecular Weight: 404.549

Synonyms:3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate

Chemical Property of 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate

There total 2 articles about 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

allyl 4-(allyloxy)-3-methoxybenzoate (1393710-66-1) + 2-hydroxyethanethiol (60-24-2) → 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate (1584677-19-9)

Guidance literature:

In neat (no solvent); UV-irradiation;

DOI:10.1039/c3gc42613k

Reference yield:

3-methoxy-4-hydroxybenzoic acid (121-34-6) → 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate (1584677-19-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / ethanol / 0.17 h / Cooling with ice

1.2: 168 h / 0 - 20 °C

2.1: neat (no solvent) / UV-irradiation

With potassium carbonate; In ethanol;

DOI:10.1039/c3gc42613k

Reference yield: 93.0%

3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate (1584677-19-9) → 3-((2-aminoethyl)thio)propyl-4-(3-((2aminoethyl)thio) propoxy)-3-methoxybenzoate (1584677-22-4)

Guidance literature:

With 2-mercaptoethylamine hydrochloride; In methanol; UV-irradiation;

DOI:10.1039/c3gc42613k

upstream raw materials:

allyl 4-(allyloxy)-3-methoxybenzoate

2-hydroxyethanethiol

3-methoxy-4-hydroxybenzoic acid

Downstream raw materials:

3-((2-aminoethyl)thio)propyl-4-(3-((2aminoethyl)thio) propoxy)-3-methoxybenzoate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1584677-19-9 3-((2-hydroxyethyl)thio)propyl-4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzoate

Send

Send

Metric Ton KG G Pound L ML

Send

Send