C₆H₉BrO

Base Information

• Chemical Name: C₆H₉BrO
• CAS No.: 1450812-67-5
• Molecular Formula: C₆H₉BrO
• Molecular Weight: 177.041
• Mol file: 1450812-67-5.mol

Synonyms:C₆H₉BrO

Chemical Property of C₆H₉BrO

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₆H₉BrO

There total 4 articles about C₆H₉BrO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C13H13BrO2 (1450812-66-4) → C6H9BrO (1450812-67-5)

Guidance literature:

With sodium methylate; In methanol; at 0 - 20 ℃; for 5h;

DOI:10.1002/anie.201207173

Reference yield:

4-benzoyloxycyclohexanone (23510-95-4) → C6H9BrO (1450812-67-5)

Guidance literature:

Multi-step reaction with 2 steps

1: triphenyl phosphite; bromine; triethylamine / dichloromethane / 20 h / -60 - 20 °C / Inert atmosphere; Reflux

2: sodium methylate / methanol / 5 h / 0 - 20 °C

With triphenyl phosphite; bromine; sodium methylate; triethylamine; In methanol; dichloromethane;

DOI:10.1002/anie.201207173

Reference yield:

4-benzoyloxycyclohexanol (6308-92-5) → C6H9BrO (1450812-67-5)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 5 h

2: triphenyl phosphite; bromine; triethylamine / dichloromethane / 20 h / -60 - 20 °C / Inert atmosphere; Reflux

3: sodium methylate / methanol / 5 h / 0 - 20 °C

With triphenyl phosphite; bromine; sodium methylate; triethylamine; pyridinium chlorochromate; In methanol; dichloromethane;

DOI:10.1002/anie.201207173

upstream raw materials:

C₁₃H₁₃BrO₂

1,4-Cyclohexanediol

4-benzoyloxycyclohexanol

4-benzoyloxycyclohexanone

Downstream raw materials:

C₈H₁₁BrO₂

C₁₉H₁₉NO