N-(Benzyloxycarbonyl)dithioglycin propylester

Base Information

• Chemical Name: N-(Benzyloxycarbonyl)dithioglycin propylester
• CAS No.: 140903-20-4
• Molecular Formula: C₁₃H₁₇NO₂S₂
• Molecular Weight: 283.415
• Mol file: 140903-20-4.mol

Synonyms:N-(Benzyloxycarbonyl)dithioglycin propylester

Chemical Property of N-(Benzyloxycarbonyl)dithioglycin propylester

Chemical Property:

Purity/Quality:

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Technology Process of N-(Benzyloxycarbonyl)dithioglycin propylester

There total 2 articles about N-(Benzyloxycarbonyl)dithioglycin propylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(Benzyloxycarbonylamino)thioacetimidsaeure-propylester hydrochlorid (140903-15-7) → N-(Benzyloxycarbonyl)dithioglycin propylester (140903-20-4)

Guidance literature:

With pyridine; hydrogen sulfide; In tetrahydrofuran; at 0 ℃; for 3h;

Reference yield:

phenylmethyl cyanomethylcarbamate (3589-41-1) → N-(Benzyloxycarbonyl)dithioglycin propylester (140903-20-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / gaseous HCl / diethyl ether / -5 °C

2: 94 percent / gaseous H₂S, pyridine / tetrahydrofuran / 3 h / 0 °C

With pyridine; hydrogenchloride; hydrogen sulfide; In tetrahydrofuran; diethyl ether;

upstream raw materials:

(Benzyloxycarbonylamino)thioacetimidsaeure-propylester hydrochlorid

phenylmethyl cyanomethylcarbamate

Refernces