Technology Process of C10H15NO3S
There total 8 articles about C10H15NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 ℃;
Inert atmosphere;
DOI:10.1002/chem.201001402
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2: 10% palladium on activated carbon; hydrogen / ethanol / 20 °C
3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere
With
1H-imidazole; 10% palladium on activated carbon; tetrabutyl ammonium fluoride; hydrogen; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201001402
- Guidance literature:
-
Multi-step reaction with 6 steps
1: boron tribromide / dichloromethane / -20 - 20 °C / Inert atmosphere
2: sodium azide / water; N,N-dimethyl-formamide / 20 - 90 °C / Inert atmosphere
3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
4: 10% palladium on activated carbon; hydrogen / ethanol / 20 °C
5: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere
With
1H-imidazole; sodium azide; 10% palladium on activated carbon; tetrabutyl ammonium fluoride; hydrogen; boron tribromide; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201001402
