(R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

Base Information

Chemical Name:(R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate
CAS No.:211623-25-5
Molecular Formula:C₃₂H₂₉N₃O₅S₃
Molecular Weight:631.797
Hs Code.:

Synonyms:(R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

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Chemical Property of (R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

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Technology Process of (R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

There total 6 articles about (R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 211623-24-4
(2S,4S,5R,6R)-6-Allyloxycarbonylamino-3,3-dimethyl-4,7-dioxo-4λ⁴-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

: 211623-25-5
(R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

Guidance literature:: In toluene; Heating;
DOI:10.1021/ja980195z

Reference yield: 91.0%

: 947589-45-9
benzhydryl 6-(allyloxycarbonylamino)penicillinate-1-oxide

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 211623-25-5
(R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

Guidance literature:: With magnesium sulfate; In 1,4-dioxane; at 110 ℃; for 14h;
DOI:10.1021/acs.jmedchem.0c00127

Reference yield:

: 47547-28-4,78184-79-9
6-aminopenicillanic acid diphenylmethyl ester

: 211623-25-5
(R)-benzhydryl 2-((2R,3R)-3-(allyloxycarbonyl)amino-2-(benzo[d]thiazol-2-yldisulfanyl)-4-oxoazetidin-1-yl)-3-methylbut-3-enoate

Guidance literature:: Multi-step reaction with 3 steps

2: MCPBA

3: toluene / Heating

With 3-chloro-benzenecarboperoxoic acid; In toluene;
DOI:10.1016/S0960-894X(99)00325-X