N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

Base Information

Chemical Name:N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide
CAS No.:787629-27-0
Molecular Formula:C₄₂H₅₄N₄O₁₂
Molecular Weight:806.91
Hs Code.:

Synonyms:N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

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Chemical Property of N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

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Technology Process of N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

There total 5 articles about N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 787629-22-5
N,N'-di-((2-methoxy-3-methoxycarbonylbenzoyl)amino) 4,6-dioctyloxy-iso-phthalamide

: 787629-27-0
N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; for 5h; Heating;
DOI:10.1021/ja047436p

Reference yield:

: 107020-28-0
2-methoxy-3-methoxycarbonylbenzoyl chloride

: 787629-27-0
N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.59 g / pyridine; N,N-dimethyl-4-aminopyridine / 2 h / 20 °C

2: 90 percent / aq. LiOH / tetrahydrofuran / 5 h / Heating

With pyridine; dmap; lithium hydroxide; In tetrahydrofuran;
DOI:10.1021/ja047436p

Reference yield:

: 267897-57-4
dimethyl 4,6-bis(octyloxy)-1,3-benzenedicarboxylate

: 787629-27-0
N,N'-di-(3-hydroxycarbonyl-2-methoxy)benzoyl 4,6-dioctyloxy-iso-phthalohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / hydrazine hydrate / 10 h / Heating

2: 1.59 g / pyridine; N,N-dimethyl-4-aminopyridine / 2 h / 20 °C

3: 90 percent / aq. LiOH / tetrahydrofuran / 5 h / Heating

With pyridine; dmap; lithium hydroxide; hydrazine hydrate; In tetrahydrofuran;
DOI:10.1021/ja047436p