Technology Process of C29H30N2O5
There total 13 articles about C29H30N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H28N2O6;
With
borane-THF;
In
tetrahydrofuran;
at 0 ℃;
for 1.5h;
With
hydrogenchloride;
In
water;
at 0 ℃;
for 0.5h;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene / 36 h / 150 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
2.2: 2.5 h / -78 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / -5 °C
5.1: borane-THF / tetrahydrofuran / 1.5 h / 0 °C
5.2: 0.5 h / 0 °C
With
borane-THF; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1H-imidazole; sodium hydride / tetrahydrofuran; mineral oil / 0 - 25 °C
1.2: 1 h / 0 - 25 °C
1.3: 1 h / 0 - 25 °C
2.1: toluene / 36 h / 150 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
3.2: 2.5 h / -78 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / -5 °C
6.1: borane-THF / tetrahydrofuran / 1.5 h / 0 °C
6.2: 0.5 h / 0 °C
With
1H-imidazole; borane-THF; tetrabutyl ammonium fluoride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1021/ja500548e
