C₂₄H₃₇ClO₅Si

Base Information

Chemical Name:C₂₄H₃₇ClO₅Si
CAS No.:1388153-30-7
Molecular Formula:C₂₄H₃₇ClO₅Si
Molecular Weight:469.093
Hs Code.:

C<sub>24</sub>H<sub>37</sub>ClO<sub>5</sub>Si

Synonyms:C₂₄H₃₇ClO₅Si

Suppliers and Price of C₂₄H₃₇ClO₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₃₇ClO₅Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₃₇ClO₅Si

There total 16 articles about C₂₄H₃₇ClO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₂₄H₃₈O₆Si

: 1388153-30-7
C₂₄H₃₇ClO₅Si

Guidance literature:: With N-chloro-succinimide; triphenylphosphine; methyloxirane; In dichloromethane; at 0 ℃; for 0.75h;
DOI:10.1021/ja305864z

Reference yield:

: C₂₆H₄₀O₆Si

: 1388153-30-7
C₂₄H₃₇ClO₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

2.2: -20 °C / Molecular sieve

3.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

With titanium(IV) isopropylate; N-chloro-succinimide; (-)-diethyl tartrate; diisobutylaluminium hydride; triphenylphosphine; methyloxirane; In hexane; dichloromethane; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388153-30-7
C₂₄H₃₇ClO₅Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 2 h / -78 - 0 °C

4.1: tetrahydrofuran / 0.5 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

6.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C

6.2: 1 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

8.2: -20 °C / Molecular sieve

9.1: N-chloro-succinimide; triphenylphosphine; methyloxirane / dichloromethane / 0.75 h / 0 °C

With titanium(IV) isopropylate; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; (-)-diethyl tartrate; camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triethylamine; triphenylphosphine; methyloxirane; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ja305864z