acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

Base Information

Chemical Name:acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline
CAS No.:181708-20-3
Molecular Formula:C₃₂H₃₂N₂
Molecular Weight:444.619
Hs Code.:

Synonyms:acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

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Chemical Property of acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

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Technology Process of acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

There total 1 articles about acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.1%

: 6310-21-0
2-(1,1-dimethylethyl)-benzenamine

: 82-86-0
acenaphthene quinone

: 181708-20-3
acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

Guidance literature:: With formic acid; In methanol; for 19h;
DOI:10.1021/ja000893v

Reference yield: 94.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 181708-20-3
acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

: ([C₆H₄C(CH₃)3N]2C₁₂H₆NiBr₂)2*CH₂Cl₂

Guidance literature:: In dichloromethane; (Ar); mixt. of Ni salt and the ligand stirred in CH2Cl2 at room temp. for 16 h; the suspn. filtered, the filtrate collected, the solvent removed, the residue washed with ether;
DOI:10.1016/S0022-328X(01)01340-7

Reference yield: 85.6%

: Pd(methyl)2(1,5-cyclooctadiene)

: 181708-20-3
acenaphthylene-(1,2-diylidene)bis-2-methoxyaniline

: Pd(CH₃)2C₆H₄(C₄H₉)NC₁₀H₆C₂NC₆H₄(C₄H₉)

Guidance literature:: In diethyl ether; Pd-complex was cooled to -30-40°C, solid was dissolved in ether,ligand in ether was added, warmed to 0°C, stirred for 2 h, stored at -30°C overnight; filtered, dried in vacuo, solvent was evapd. under vac., washed with hexane, dried in vacuo; elem. anal.;
DOI:10.1021/ja000893v