7-methoxy-2-phenylbenzothiazoles

Base Information

• Chemical Name: 7-methoxy-2-phenylbenzothiazoles
• CAS No.: 1146961-24-1
• Molecular Formula: C₁₄H₁₁NOS
• Molecular Weight: 241.313
• Mol file: 1146961-24-1.mol

Synonyms:7-methoxy-2-phenylbenzothiazoles

Chemical Property of 7-methoxy-2-phenylbenzothiazoles

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 7-methoxy-2-phenylbenzothiazoles

There total 4 articles about 7-methoxy-2-phenylbenzothiazoles which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N-(3-methoxyphenyl)benzothioamide → 7-methoxy-2-phenylbenzothiazoles (1146961-24-1) + 5-methoxy-2-phenyl-1,3-benzothiazole

Guidance literature:

With p-nitrobenzene iodide; Oxone; trifluorormethanesulfonic acid; at 20 ℃; for 6h; Green chemistry;

DOI:10.1021/jo501216h

Reference yield: 88.0%

N-(3-methoxyphenyl)benzothioamide → 7-methoxy-2-phenylbenzothiazoles (1146961-24-1)

Guidance literature:

With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Irradiation;

DOI:10.1021/ol2028866

Reference yield: 85.0%

→ 7-methoxy-2-phenylbenzothiazoles (1146961-24-1)

Guidance literature:

With C₅H₈NO₂^(1-)*Li⁽¹⁺⁾*NiCl₂; potassium thioacyanate; sodium hydroxide; In water; at 100 ℃; for 0.5h; Microwave irradiation;

upstream raw materials:

N-(3-methoxyphenyl)benzamide