C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

Base Information

Chemical Name:C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)
CAS No.:1366231-89-1
Molecular Formula:C₅₃H₁₀₅N₄O₈*I
Molecular Weight:1053.34
Hs Code.:

C<sub>53</sub>H<sub>105</sub>N<sub>4</sub>O<sub>8</sub><sup>(1+)</sup>*I<sup>(1-)</sup>

Synonyms:C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

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Chemical Property of C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

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Technology Process of C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

There total 6 articles about C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1366231-88-0
C₆₁H₁₁₃N₄O₁₂⁽¹⁺⁾*I^(1-)

: 1366231-89-1
C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

Guidance literature:: C₆₁H₁₁₃N₄O₁₂⁽¹⁺⁾*I^(1-); With methanol; potassium carbonate; at 25 ℃; for 0.5h; pH=~ 9;

In methanol;

Reference yield:

: 93551-68-9
N¹,N¹-dihexadecyl-1,2-ethanediamine

: 1366231-89-1
C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Cooling with ice

1.2: 12 h / 25 °C

2.1: hydrogenchloride; hydrogen / 10 wt% Pd(OH)2 on carbon / water; methanol / 14 h / 25 °C / 1520.1 Torr

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Cooling with ice

3.2: 12 h / 25 °C

4.1: chloroform; methanol / 6 h / 20 °C

5.1: potassium carbonate; methanol / 0.5 h / 25 °C / pH ~ 9

5.2: Amberlite IR₁₂₀ (H⁺)

With hydrogenchloride; methanol; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 10 wt% Pd(OH)2 on carbon; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: [5-benzyloxycarbonylamino-5-(2-dihexadecylamino-ethylcarbamoyl)-pentyl]-carbamic acid tert-butyl ester

: 1366231-89-1
C₅₃H₁₀₅N₄O₈⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; hydrogen / 10 wt% Pd(OH)2 on carbon / water; methanol / 14 h / 25 °C / 1520.1 Torr

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Cooling with ice

2.2: 12 h / 25 °C

3.1: chloroform; methanol / 6 h / 20 °C

4.1: potassium carbonate; methanol / 0.5 h / 25 °C / pH ~ 9

4.2: Amberlite IR₁₂₀ (H⁺)

With hydrogenchloride; methanol; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 10 wt% Pd(OH)2 on carbon; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;