1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

Base Information

Chemical Name:1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate
CAS No.:1258949-02-8
Molecular Formula:C₂₄H₁₇N₅O₈
Molecular Weight:503.428
Hs Code.:

Synonyms:1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

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Chemical Property of 1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

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Technology Process of 1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

There total 6 articles about 1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.03%

: 1258948-96-7
N'-(1-chlorovinyloxy)-1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbohydrazide

: 1258949-02-8
1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

Guidance literature:: With silver nitrate; In acetonitrile; at 20 ℃;
DOI:10.2174/1573406411006040211

Reference yield:

: C₂₂H₁₃ClN₂O₄

: 1258949-02-8
1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 6 h / Reflux

2: triethylamine / benzene / 10 h / Reflux

3: silver nitrate / acetonitrile / 20 °C

With hydrazine hydrate; silver nitrate; triethylamine; In ethanol; acetonitrile; benzene;
DOI:10.2174/1573406411006040211

Reference yield:

: 1258948-84-3
3-nirophenone-2-phenyl-5-indolecarboxylic acid

: 1258949-02-8
1-(2-(1-(3-nitrobenzoyl)-2-phenyl-1H-indole-5-carbonyl)hydrazinyloxy)vinyl nitrate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 4 h / Reflux

2: hydrazine hydrate / ethanol / 6 h / Reflux

3: triethylamine / benzene / 10 h / Reflux

4: silver nitrate / acetonitrile / 20 °C

With thionyl chloride; hydrazine hydrate; silver nitrate; triethylamine; In ethanol; acetonitrile; benzene;
DOI:10.2174/1573406411006040211