1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

Base Information

Chemical Name:1H-cyclobutanaphthalen-1-yl p-toluenesulfonate
CAS No.:85924-87-4
Molecular Formula:C₁₈H₁₄O₃S
Molecular Weight:310.373
Hs Code.:

1H-cyclobuta<de>naphthalen-1-yl p-toluenesulfonate

Synonyms:1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

Chemical Property:

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Technology Process of 1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

There total 5 articles about 1H-cyclobutanaphthalen-1-yl p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54125-11-0
1-Bromo-1H-cyclobutanaphthalene

: 16836-95-6
silver(I) 4-methylbenzenesulfonate

: 85924-87-4
1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

: 66-77-3
1-naphthaldehyde

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; at 75 ℃; for 50h;
DOI:10.1021/ja00357a022

Reference yield:

: 24973-91-9
1H-Cyclobutanaphthalene

: 85924-87-4
1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

2: 60 percent Turnov_. / hexamethylphosphoric acid triamide / 50 h / 75 °C

With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ja00357a022

Reference yield:

: 85924-73-8
C₁₁H₇Li

: 85924-87-4
1H-cyclobutanaphthalen-1-yl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 25 mg / tetrahydrofuran / 0.17 h / -78 °C

2: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

3: 60 percent Turnov_. / hexamethylphosphoric acid triamide / 50 h / 75 °C

With N-Bromosuccinimide; Perbenzoic acid; In tetrahydrofuran; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ja00357a022