4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate

Base Information

• Chemical Name: 4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate
• CAS No.: 1092166-69-2
• Molecular Formula: C₂₅H₃₄O₆S
• Molecular Weight: 462.607

Synonyms:4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate

Chemical Property of 4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate

Chemical Property:

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Technology Process of 4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate

There total 1 articles about 4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

4-[3-(2-butoxy-4-hydroxymethyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate (1092166-68-1) → 4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate (1092166-69-2)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 15h;

Reference yield: 62.0%

4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate (1092166-69-2) + methyl 2-methoxy-2-(triphenylphosphonium)acetate chloride → (Z)-3-(4-{3-[4-(butane-1-sulfonyloxy)-3-methoxy-phenyl]-propyl}-3-butoxy-phenyl)-2-methoxy-methyl acrylate (1092166-70-5)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 60 ℃; for 6h;

Reference yield: 62.0%

4-[3-(2-butoxy-4-formyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate (1092166-69-2) + 1-methoxycarbonyl-ethyl-triphenyl phosphonium chloride (2535-91-3) → (Z)-3-(4-{3-[4-(butane-1-sulfonyloxy)-3-methoxy-phenyl]-propyl}-3-butoxy-phenyl)-2-methyl-methyl acrylate (1092166-74-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 60 ℃; for 6h;

upstream raw materials:

4-[3-(2-butoxy-4-hydroxymethyl-phenyl)-propyl]-2-methoxy-phenyl 1-butane sulfonate

Downstream raw materials:

(Z)-3-(4-{3-[4-(butane-1-sulfonyloxy)-3-methoxy-phenyl]-propyl}-3-butoxy-phenyl)-2-ethoxy-ethyl acrylate

(Z)-3-(4-{3-[4-(butane-1-sulfonyloxy)-3-methoxy-phenyl]-propyl}-3-butoxy-phenyl)-2-methoxy-methyl acrylate

(Z)-3-(4-{3-[4-(butane-1-sulfonyloxy)-3-methoxy-phenyl]-propyl}-3-butoxy-phenyl)-2-methyl-methyl acrylate

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