1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

Base Information

Chemical Name:1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione
CAS No.:205653-99-2
Molecular Formula:C₂₂H₂₅NO₁₀
Molecular Weight:463.441
Hs Code.:

Synonyms:1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

Suppliers and Price of 1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

There total 2 articles about 1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 106331-50-4
1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

: 205653-98-1
3-methoxy-4-hydroxyethoxy-5-nitrobenzaldehyde

: 205653-99-2
1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

Guidance literature:: With 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; triethylamine; at 60 ℃; for 16h;
DOI:10.1021/jm980046r

Reference yield:

: 6635-20-7
isonitrovanillin

: 205653-99-2
1-(3-methoxy-4-hydroxyethoxy-5-nitrophenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanedione

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / K₂CO₃, 18-crown-6 / dimethylformamide / 48 h / 80 °C

2: 60 percent / 3-benzyl-5-(2-hydroxyethyl)-4-methylthiazolium chloride, triethylamine / 16 h / 60 °C

With 18-crown-6 ether; 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; potassium carbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm980046r