Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo- (9CI)

Base Information

• Chemical Name: Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo- (9CI)
• CAS No.: 285996-76-1
• Molecular Formula: C₁₂H₁₉NO₅
• Molecular Weight: 257.287
• Hs Code.: 2924299090
• Mol file: 285996-76-1.mol

Synonyms:1-tert-Butoxycarbonylamino-4-oxocyclohexanecarboxylicacid

Chemical Property of Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo- (9CI)

Chemical Property:

• PSA: 96.19000
• LogP: 1.68200
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-(BOC-amino)-4-oxocyclohexanecarboxylicacid 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo- (9CI)

There total 1 articles about Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethoxy)carbonyl]amino]-4-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-((tert-butoxycarbonyl)amino)-4-oxocyclohexanecarboxylic acid (285996-76-1)

Guidance literature:

Reference yield:

1-((tert-butoxycarbonyl)amino)-4-oxocyclohexanecarboxylic acid (285996-76-1) → C13H21F2NO4

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; hexane / 20 °C

2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / ethanol / 16 h / 20 °C

With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In methanol; ethanol; hexane;

Reference yield:

1-((tert-butoxycarbonyl)amino)-4-oxocyclohexanecarboxylic acid (285996-76-1) → C19H25F2NO4

Guidance literature:

Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2.1: diethylamino-sulfur trifluoride / dichloromethane / 20 °C

2.2: 20 °C

With diethylamino-sulfur trifluoride; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;