Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

Base Information

• Chemical Name: Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)
• CAS No.: 947683-68-3
• Molecular Formula: C₆₇H₈₀N₄NiSi
• Molecular Weight: 1028.17
• Mol file: 947683-68-3.mol

Synonyms:Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

Chemical Property of Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

There total 1 articles about Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(C₂Si(CH₃)3)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Ni((C(CH3)3)2C6H3CC4NH2CHC4NH(O3SCF3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-64-9) + trimethylsilylacetylene (1066-54-2) → Ni((C(CH3)3)2C6H3CC4NH2CHC4NH(C2Si(CH3)3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-68-3)

Guidance literature:

With CuI; Pd(P(C₆H₅)3)4; N(C₂H₅)3; In tetrahydrofuran; toluene; reaction at 70 °C for 3 h;

DOI:10.1002/anie.200700550

Reference yield:

Ni((C(CH3)3)2C6H3CC4NH2CHC4NH(C2Si(CH3)3)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2) (947683-68-3) → Ni((C(CH3)3)2C6H3CC4NH2CHC4NH(C2H)C(C6H3(C(CH3)3)2)C4NH2C(C6H3(C(CH3)3)2)C4NH2)

Guidance literature:

With K₂CO₃; In tetrahydrofuran; methanol; reaction at room temp. for 2 h;

DOI:10.1002/anie.200700550

upstream raw materials:

Ni((C(CH₃)3)2C₆H₃CC₄NH₂CHC₄NH(O₃SCF₃)C(C₆H₃(C(CH₃)3)2)C₄NH₂C(C₆H₃(C(CH₃)3)2)C₄NH₂)

trimethylsilylacetylene