α-chloro-β-(1-adamantyl)styrene

Base Information

Chemical Name:α-chloro-β-(1-adamantyl)styrene
CAS No.:74203-38-6
Molecular Formula:C₁₈H₂₁Cl
Molecular Weight:272.818
Hs Code.:

Synonyms:α-chloro-β-(1-adamantyl)styrene

Suppliers and Price of α-chloro-β-(1-adamantyl)styrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of α-chloro-β-(1-adamantyl)styrene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of α-chloro-β-(1-adamantyl)styrene

There total 4 articles about α-chloro-β-(1-adamantyl)styrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 935-56-8
1-chloroadamantane

: 2170-06-1
1-Phenyl-2-(trimethylsilyl)acetylene

: 74203-38-6
α-chloro-β-(1-adamantyl)styrene

Guidance literature:: zinc(II) chloride; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1021/jo01306a004

Reference yield:

: 935-56-8
1-chloroadamantane

: 2170-06-1
1-Phenyl-2-(trimethylsilyl)acetylene

: Z-2-adamantyl-1-chloro-1-phenylethene

: 74203-38-6
α-chloro-β-(1-adamantyl)styrene

Guidance literature:: With zinc(II) chloride; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/acs.joc.5b00456

Reference yield:

: 770-71-8
1-adamantanemethanol

: Z-2-adamantyl-1-chloro-1-phenylethene

: 74203-38-6
α-chloro-β-(1-adamantyl)styrene

Guidance literature:: Multi-step reaction with 3 steps

1.1: Dess-Martin periodane / dichloromethane; water / 0.5 h / 25 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 1 h / -35 - 0 °C / Inert atmosphere

2.3: 0.5 h / 0 °C / Inert atmosphere

3.1: pentan-3-one / 20 °C / UV-irradiation; Inert atmosphere

With Dess-Martin periodane; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; pentan-3-one;
DOI:10.1021/acs.joc.5b00456