(1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

Base Information

Chemical Name:(1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde
CAS No.:863639-86-5
Molecular Formula:C₂₂H₃₆O₃Si
Molecular Weight:376.612
Hs Code.:

Synonyms:(1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

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Chemical Property of (1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

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Technology Process of (1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

There total 1 articles about (1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863639-93-4
2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-((1S,6R)-6-hydroxymethyl-6-methyl-cyclohex-3-enyl)-ethyl]-cyclohex-2-enol

: 863639-86-5
(1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; In dichloromethane;
DOI:10.1039/b503406j

Reference yield: 76.0%

: 863639-86-5
(1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

: 863639-93-4
2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-((1S,6R)-6-hydroxymethyl-6-methyl-cyclohex-3-enyl)-ethyl]-cyclohex-2-enol

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; tert-butyl alcohol; at 0 ℃; for 3.5h;
DOI:10.1039/b503406j

Reference yield:

: 863639-86-5
(1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-oxo-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

: (1R,6S)-6-[(R)-2-(tert-Butyl-dimethyl-silanyloxy)-2-(6-hydroxy-cyclohex-1-enyl)-ethyl]-1-methyl-cyclohex-3-enecarbaldehyde

: 863639-93-4
2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-2-((1S,6R)-6-hydroxymethyl-6-methyl-cyclohex-3-enyl)-ethyl]-cyclohex-2-enol

Guidance literature:: With samarium diiodide; In tetrahydrofuran; tert-butyl alcohol; at 0 ℃; Title compound not separated from byproducts;
DOI:10.1039/b503406j