Formamide-13C,15N

Base Information

• Chemical Name: Formamide-13C,15N
• CAS No.: 285977-74-4
• Molecular Formula: CH₃NO
• Molecular Weight: 47.0232
• European Community (EC) Number: 685-233-1
• DSSTox Substance ID: DTXSID90584349
• Wikidata: Q82476000
• Mol file: 285977-74-4.mol

Synonyms:Formamide-13C,15N;285977-74-4;(15N)azanylformaldehyde;Glycine-13C,15N;FORMAMIDE-13C 15N 99% CHEMICAL PURITY&;(~13~C,~15~N)Formamide;DTXSID90584349;HY-Y0842S2;CS-0542122;J-017136;Formamide-13C,15N, 98 atom % 15N, 99 atom % 13C, 99% (CP)

Chemical Property of Formamide-13C,15N

Chemical Property:

• Melting Point: 2-3 °C(lit.)
• Refractive Index: 1.369
• Boiling Point: 210 °C(lit.)
• Flash Point: 150 °C
• PSA: 44.08000
• Density: 1.183 g/mL at 25 °C
• LogP: 0.25120
• XLogP3: -0.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 47.021853449
• Heavy Atom Count: 3
• Complexity: 12.3

Purity/Quality:

98% by CP; 99% atom 13C; 98% atom 15N ^*data from raw suppliers

Formamide-13C,15N ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 61
• Safety Statements: 53-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=O)N
• Isomeric SMILES: [13CH](=O)[15NH2]
• Uses: Formamide-13C, 15N is labelled Formamide ( F691780) and a useful research chemical used in synthesis of [14C]-, [13C4]-, and [13C4,15N2]-5-amino-4-iodopyrimidine. Formamide (F691780 ) is a compound that is used in biochemistry to prevent RNA samples from degradation due to RNAses. Formamide (F691780 CAS# 75-12-7) is also used as a plasticizer to prepare thermoplastic starch (TPS), a special type of starch that can be mixed with other synthetic polymers because of its unique ability to “flow”

Technology Process of Formamide-13C,15N

There total 2 articles about Formamide-13C,15N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(13C)-formic acid (1633-56-3) → [13C,15N]formamide (285977-74-4)

Guidance literature:

With urea-15N₂; at 150 ℃; for 4h;

DOI:10.1021/ja012253d

Reference yield:

urea-15N2 (2067-80-3) + (13C)-formic acid (1633-56-3) → [13C,15N]formamide (285977-74-4)

Guidance literature:

at 150 ℃; for 4h;

DOI:10.1016/S0040-4039(00)01731-7

Reference yield:

2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) + [13C,15N]formamide (285977-74-4) → 2-13C-1,3-15N-4,5-diphenylimidazole (328084-17-9)

Guidance literature:

With ammonia; at 180 ℃; for 3h;

DOI:10.1016/S0040-4039(00)01731-7

upstream raw materials:

urea-15N₂

(¹³C)-formic acid

Downstream raw materials:

2-13C-1,3-15N-4,5-diphenylimidazole