benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside
CAS No.:83055-36-1
Molecular Formula:C₂₁H₂₉N₅O₇
Molecular Weight:463.491
Hs Code.:

benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O-<D-1-(methoxycarbonyl)ethyl>-α-D-galactopyranoside

Synonyms:benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

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Chemical Property of benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

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Technology Process of benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

There total 4 articles about benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 83055-32-7
benzyl 2,6-di(acetamido)-2,6-dideoxy-4-O-mesyl-3-O--α-D-glucopyranoside

: 83055-36-1
benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; for 6.5h; Heating;
DOI:10.1016/S0008-6215(00)80688-6

Reference yield:

: 77268-46-3
benzyl 2-acetamido-6-azido-2,6-dideoxy-3-O--α-D-glucopyranoside

: 83055-36-1
benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) hydrogen / 1.) 10 percent Pd-C / 1.) methanol, room temperature, 40 min; 2.) methanol, room temperature, 30 min

2: 92 percent / pyridine / 0 °C

3: 49 percent / sodium azide / dimethylformamide / 6.5 h / 100 °C / Heating

With pyridine; sodium azide; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80688-6

Reference yield:

: 74221-00-4
benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

: 83055-36-1
benzyl 2,6-di(acetamido)-4-azido-2,4,6-trideoxy-3-O--α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / sodium azide / dimethylformamide / 5 h / 80 °C / Heating

2: 1.) hydrogen / 1.) 10 percent Pd-C / 1.) methanol, room temperature, 40 min; 2.) methanol, room temperature, 30 min

3: 92 percent / pyridine / 0 °C

4: 49 percent / sodium azide / dimethylformamide / 6.5 h / 100 °C / Heating

With pyridine; sodium azide; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80688-6