octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

Base Information

Chemical Name:octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene
CAS No.:110684-83-8
Molecular Formula:C₂₆H₃₂O₃S
Molecular Weight:424.604
Hs Code.:

Synonyms:octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

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Technology Process of octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

There total 6 articles about octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 110684-82-7
4-(1,1-dimethylethyl)-1-(phenylethynyl)-2-<2-(phenylseleno)-2-(phenylsulfonyl)ethyl>cyclohexan-1-ol

: 110684-83-8
octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); triphenylstannane; In benzene; for 15h; Heating;
DOI:10.1021/jo00231a021

Reference yield:

: 4147-00-6
4-tert-butyl-1-(1-pyrrolidinyl)cyclohexene

: 110684-83-8
octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / tetrahydrofuran / 3 h / Ambient temperature

2: 1.) n-butyllithium / 1.) THF, hexanes, -78 deg C, 15 min, 2.) THF, hexanes, -78 deg C, 2 h

3: 65 percent / triphenyltin hydride, AIBN / benzene / 15 h / Heating

With n-butyllithium; 2,2'-azobis(isobutyronitrile); triphenylstannane; In tetrahydrofuran; benzene;
DOI:10.1021/jo00231a021

Reference yield:

: 5535-48-8
PVS

: 110684-83-8
octahydro-7a-hydroxy-5-(1,1-dimethylethyl)-1-(phenylmethylene)-2-(phenylsulfonyl)-1H-indene

Guidance literature:: Multi-step reaction with 5 steps

1: CCl₄ / 18 h / Heating

2: triethylamine / benzene / 18 h / Ambient temperature

3: 98 percent / tetrahydrofuran / 3 h / Ambient temperature

4: 1.) n-butyllithium / 1.) THF, hexanes, -78 deg C, 15 min, 2.) THF, hexanes, -78 deg C, 2 h

5: 65 percent / triphenyltin hydride, AIBN / benzene / 15 h / Heating

With n-butyllithium; 2,2'-azobis(isobutyronitrile); triphenylstannane; triethylamine; In tetrahydrofuran; tetrachloromethane; benzene;
DOI:10.1021/jo00231a021