(E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

Base Information

Chemical Name:(E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate
CAS No.:1318796-35-8
Molecular Formula:C₁₂H₁₇N₃O₅
Molecular Weight:283.284
Hs Code.:

Synonyms:(E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

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Technology Process of (E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

There total 3 articles about (E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1318796-77-8
dimethyl 2-(cyclohexyloxyimino)succinate

: 1318796-35-8
(E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

Guidance literature:: With p-nitrobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at -20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c1cc11683e

Reference yield:

: 25007-54-9
Dimethyl 2-oxosuccinate

: 1318796-35-8
(E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h / 20 °C / Inert atmosphere

2: p-nitrobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere

With pyridine; p-nitrobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1039/c1cc11683e

Reference yield:

: 54488-64-1
O-cyclohexylhydroxylamine hydrochloride

: 1318796-35-8
(E)-dimethyl 2-(cyclohexyloxyimino)-3-diazosuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h / 20 °C / Inert atmosphere

2: p-nitrobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / -20 °C / Inert atmosphere

With pyridine; p-nitrobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile;
DOI:10.1039/c1cc11683e