-2 dimethyl-4,4 oxazoline-2

Base Information

• Chemical Name: -2 dimethyl-4,4 oxazoline-2
• CAS No.: 112041-39-1
• Molecular Formula: C₂₀H₂₄N₂O₅
• Molecular Weight: 372.421

Synonyms:-2 dimethyl-4,4 oxazoline-2

Chemical Property of -2 dimethyl-4,4 oxazoline-2

Chemical Property:

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Technology Process of -2 dimethyl-4,4 oxazoline-2

There total 1 articles about -2 dimethyl-4,4 oxazoline-2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<(methoxy-2 pyridyl)-4>-2 dimethyl-4,4 oxazoline-2 (111424-19-2) + 2,5-dimethoxybenzaldehyde (93-02-7) → -2 dimethyl-4,4 oxazoline-2 (112041-39-1)

Guidance literature:

With methyllithium; Yield given. Multistep reaction; 1.) THF, ether, 0 deg C, 1 h, 2.) rt, 18 h;

Reference yield: 92.0%

-2 dimethyl-4,4 oxazoline-2 (112041-39-1) → 1,3-dihydro-3-(2',5'-dimethoxyphenyl)-4 methoxy-(3H)-furo<3,4-c>pyridin-1-one (115843-04-4)

Guidance literature:

With acetic acid; for 24h; Ambient temperature; PCC in CH₂Cl₂, 3 d, RT;

DOI:10.1016/0223-5234(88)90175-4

Reference yield: 89.0%

-2 dimethyl-4,4 oxazoline-2 (112041-39-1) → (dimethoxy-2',5' phenyl)-3-3H,5H-furo<3,4-c>pyridin dione 1,4 (112039-66-4)

Guidance literature:

With hydrogenchloride; for 3h; Heating;

upstream raw materials:

<(methoxy-2 pyridyl)-4>-2 dimethyl-4,4 oxazoline-2

2,5-dimethoxybenzaldehyde

Downstream raw materials:

(dimethoxy-2',5' phenyl)-3-3H,5H-furo<3,4-c>pyridin dione 1,4

3-(2,5-Dimethoxy-benzoyl)-2-oxo-1,2-dihydro-pyridine-4-carboxylic acid

1,3-dihydro-3-(2',5'-dimethoxyphenyl)-4 methoxy-(3H)-furo<3,4-c>pyridin-1-one

2-[3-(2,5-Dimethoxy-benzoyl)-2-methoxy-pyridin-4-yl]-4,4-dimethyl-4H-oxazol-5-one

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