geranylgeranyl acetate

Base Information

Chemical Name:geranylgeranyl acetate
CAS No.:61691-98-3
Molecular Formula:C₂₂H₃₆O₂
Molecular Weight:332.527
Hs Code.:

Synonyms:geranylgeranyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of geranylgeranyl acetate

Chemical Property:

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Technology Process of geranylgeranyl acetate

There total 1 articles about geranylgeranyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 61691-98-3
geranylgeranyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) lithium biphenylide, barium iodide / 1) THF, -78 deg C, 30 min, 2) THF, a) -78 deg C, 1.5 h, b) room temperature, 16 h

2: 95 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 16 h / 23 °C

3: 100 percent / pyridine / 3 h / 23 °C

With pyridine; lithium biphenylide; barium(II) iodide; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)79008-3

Reference yield:

: 61691-98-3
geranylgeranyl acetate

: 5016-85-3,10236-16-5,76337-16-1,118100-83-7,118100-84-8,118100-94-0,118138-59-3
(all-rac,Z)-phytyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / 1.8 N HCl in pentane / pentane / 0.08 h / -78 °C

2: azoisobutyronitrile, tributyltin hydride / cyclohexane / 1 h / 75 °C

With hydrogenchloride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In cyclohexane; pentane;
DOI:10.1016/S0040-4020(01)88050-9

Reference yield:

: 61691-98-3
geranylgeranyl acetate

: C₂₇H₄₀O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: mercury ditrifluoroacetate; N,N-dimethylaniline; MeNO₂

1.2: KBr

1.3: NaOH; NaBH₄ / ethanol; CH₂Cl₂; H₂O

2.1: 62 percent / 4-(dimethylamino)pyridine; triethylamine / CH₂Cl₂ / 3 h / 20 °C

3.1: 95 percent / 4-(dimethylamino)pyridine; N,N-diisopropylethylamine / CH₂Cl₂ / 21 h / 50 - 70 °C

4.1: 96 percent / tetrabutylammonium fkuoride / tetrahydrofuran / 21 h / 60 - 70 °C

5.1: PCC; CH₃COONa / CH₂Cl₂ / 4.5 h / 0 °C

6.1: tert-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

6.2: 65 percent / tetrahydrofuran / 3 h / -78 °C

7.1: H₂ / Pd(OH)2/C / ethanol; ethyl acetate / 20 °C

7.2: O₂ / ethanol; ethyl acetate

With dmap; nitromethane; hydrogen; tert.-butyl lithium; sodium acetate; N,N-dimethyl-aniline; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; palladium dihydroxide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/np060481l