2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

Base Information

Chemical Name:2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin
CAS No.:87907-59-3
Molecular Formula:C₄₈H₆₂O₅
Molecular Weight:719.017
Hs Code.:

Synonyms:2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

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Technology Process of 2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

There total 17 articles about 2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 582-25-2
Potassium benzoate

: 87889-08-5
1-O-<(p-Methoxyphenyl)diphenylmethyl>-3-O-<(Z)-9-octadecenyl>-2-O-p-toluolsulfonyl-sn-glycerin

: 87907-59-3
2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

Guidance literature:: In dimethyl sulfoxide; at 140 ℃; for 0.5h;
DOI:10.1002/hlca.19830660423

Reference yield:

: 143-28-2,593-47-5,84286-21-5
oleoyl alcohol

: 87907-59-3
2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

Guidance literature:: Multi-step reaction with 5 steps

1: 92.8 percent / CHCl₃; pyridine / 3 h / Ambient temperature

2: 1.) 80percent NaH / 1.) DMF, 30 min, 50 deg C; 2.) 1 h, 80 deg C

3: 86.3 percent / 1 N HCl / H₂O; dioxane / 0.08 h / 90 °C

4: 85.6 percent / pyridine / Ambient temperature

5: 5.8 g / CH₂Cl₂; pyridine / 2 h / Ambient temperature

With hydrogenchloride; sodium hydride; In 1,4-dioxane; pyridine; dichloromethane; chloroform; water;
DOI:10.1002/hlca.19830660423

Reference yield:

: 112-62-9
Methyl oleate

: 87907-59-3
2-O-Benzoyl-3-O-<(p-methoxyphenyl)diphenylmethyl>-1-O-<(Z)-9-octadecenyl>-sn-glycerin

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / LiAlH₄ / diethyl ether / 1 h / Heating

2: 92.8 percent / CHCl₃; pyridine / 3 h / Ambient temperature

3: 1.) 80percent NaH / 1.) DMF, 30 min, 50 deg C; 2.) 1 h, 80 deg C

4: 86.3 percent / 1 N HCl / H₂O; dioxane / 0.08 h / 90 °C

5: 85.6 percent / pyridine / Ambient temperature

6: 5.8 g / CH₂Cl₂; pyridine / 2 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; In 1,4-dioxane; pyridine; diethyl ether; dichloromethane; chloroform; water;
DOI:10.1002/hlca.19830660423