pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone

Base Information

• Chemical Name: pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone
• CAS No.: 130583-76-5
• Molecular Formula: C₁₉H₂₀N₂O₂S
• Molecular Weight: 340.446

Synonyms:pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone

Chemical Property of pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone

Chemical Property:

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Technology Process of pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone

There total 1 articles about pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5-<<<(tert-butyl)dimethylsilyl>oxy>methylidene>pentacyclo<5.4.0.02,4.03,9.06,8>undec-10-ene (130622-13-8) + toluene-4-sulfonic acid hydrazide (1576-35-8) → pentacyclo<5.4.0.02,4.03,9.06,8>undec-10-ene-5-carboxaldehyde 4-toluenesulfonylhydrazone (130583-76-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1002/hlca.19900730506

upstream raw materials:

5-<<<(tert-butyl)dimethylsilyl>oxy>methylidene>pentacyclo<5.4.0.0^2,4.0^3,9.0^6,8>undec-10-ene

toluene-4-sulfonic acid hydrazide

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