C₃₄H₅₄O₆Si

Base Information

Chemical Name:C₃₄H₅₄O₆Si
CAS No.:1209386-11-7
Molecular Formula:C₃₄H₅₄O₆Si
Molecular Weight:586.885
Hs Code.:

C<sub>34</sub>H<sub>54</sub>O<sub>6</sub>Si

Synonyms:C₃₄H₅₄O₆Si

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Chemical Property of C₃₄H₅₄O₆Si

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Technology Process of C₃₄H₅₄O₆Si

There total 10 articles about C₃₄H₅₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1209385-74-9
C₃₄H₅₄O₅Si

: 1209386-11-7
C₃₄H₅₄O₆Si

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; D-(-)-diisopropyl tartrate; In decane; dichloromethane; at -20 ℃; for 4h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo400260m

Reference yield:

: C₁₉H₂₈O₄

: 1209386-11-7
C₃₄H₅₄O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 0.5 h / 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere

3: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve

4: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

5: dichloromethane / 0.02 h / 0 °C / Inert atmosphere

6: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; formic acid; triethylamine / 1,4-dioxane / 9.5 h / 20 °C / Inert atmosphere

7: 2,6-dimethylpyridine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

8: diisobutylaluminium hydride / dichloromethane; hexane / 0.12 h / -78 °C / Inert atmosphere

9: D-(-)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 4 h / -20 °C / Inert atmosphere; Molecular sieve

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; formic acid; L-(+)-diisopropyl tartrate; tributylphosphine; trifluorormethanesulfonic acid; sulfur trioxide pyridine complex; diisobutylaluminium hydride; D-(-)-diisopropyl tartrate; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; decane; hexane; dichloromethane; cyclohexane; 3: |Sharpless Asymmetric Epoxidation / 4: |Parikh-Doering Oxidation / 5: |Horner-Wadsworth-Emmons Olefination / 9: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo400260m

Reference yield:

: C₂₇H₃₆O₅

: 1209386-11-7
C₃₄H₅₄O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere

2: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve

3: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

4: dichloromethane / 0.02 h / 0 °C / Inert atmosphere

5: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; formic acid; triethylamine / 1,4-dioxane / 9.5 h / 20 °C / Inert atmosphere

6: 2,6-dimethylpyridine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

7: diisobutylaluminium hydride / dichloromethane; hexane / 0.12 h / -78 °C / Inert atmosphere

8: D-(-)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 4 h / -20 °C / Inert atmosphere; Molecular sieve

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; formic acid; L-(+)-diisopropyl tartrate; tributylphosphine; sulfur trioxide pyridine complex; diisobutylaluminium hydride; D-(-)-diisopropyl tartrate; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; decane; hexane; dichloromethane; 2: |Sharpless Asymmetric Epoxidation / 3: |Parikh-Doering Oxidation / 4: |Horner-Wadsworth-Emmons Olefination / 8: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo400260m