N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Base Information

Chemical Name:N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide
CAS No.:1430883-52-5
Molecular Formula:C₃₀H₄₇N₇O
Molecular Weight:521.749
Hs Code.:

Synonyms:N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

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Chemical Property of N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

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Technology Process of N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

There total 8 articles about N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-26-2
hexan-1-amine

: 1430850-15-9
N-(2-(4-(7-bromo-6-oxoheptyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

: 1430883-52-5
N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Guidance literature:: With hydrogenchloride; CYANAMID; In ethanol; water; at 95 ℃; for 3h; pH=4.3;
DOI:10.1016/j.ejmech.2012.12.005

Reference yield:

: 1430850-09-1
N-(2-(4-(6-hydroxyhexyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

: 1430883-52-5
N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Guidance literature:: Multi-step reaction with 5 steps

1: Jones reagent / acetone / 0.83 h / 0 - 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.25 h / 0 - 20 °C

3: dichloromethane; diethyl ether / 1 h / 0 °C

4: hydrogen bromide / dichloromethane; diethyl ether / 0.5 h / 0 °C

5: CYANAMID; hydrogenchloride / water; ethanol / 3 h / 95 °C / pH 4.3

With hydrogenchloride; Jones reagent; oxalyl dichloride; CYANAMID; hydrogen bromide; N,N-dimethyl-formamide; In diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.ejmech.2012.12.005

Reference yield:

: 1430850-14-8
6-(1-(2-(4-pentylbenzamido)ethyl)-1H-1,2,3-triazol-4-yl)hexanoic acid

: 1430883-52-5
N-(2-(4-(5-(2-amino-1-hexyl-1H-imidazol-4-yl)pentyl)-1H-1,2,3-triazol-1-yl)ethyl)-4-pentylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.25 h / 0 - 20 °C

2: dichloromethane; diethyl ether / 1 h / 0 °C

3: hydrogen bromide / dichloromethane; diethyl ether / 0.5 h / 0 °C

4: CYANAMID; hydrogenchloride / water; ethanol / 3 h / 95 °C / pH 4.3

With hydrogenchloride; oxalyl dichloride; CYANAMID; hydrogen bromide; N,N-dimethyl-formamide; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2012.12.005