C₃₂H₄₆O₃

Base Information

Chemical Name:C₃₂H₄₆O₃
CAS No.:1318052-37-7
Molecular Formula:C₃₂H₄₆O₃
Molecular Weight:478.715
Hs Code.:

C<sub>32</sub>H<sub>46</sub>O<sub>3</sub>

Synonyms:C₃₂H₄₆O₃

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Chemical Property of C₃₂H₄₆O₃

Chemical Property:

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Technology Process of C₃₂H₄₆O₃

There total 12 articles about C₃₂H₄₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1186505-20-3
C₃₄H₄₆O₅

: 1318052-37-7
C₃₂H₄₆O₃

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1016/j.tet.2011.05.092

Reference yield:

: 1318052-03-7
C₂₀H₃₂O

: 1318052-37-7
C₃₂H₄₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C

2.1: pyrrolidine / diethyl ether / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / 0 °C / Inert atmosphere

3.2: 8 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere

4.2: 0 - 35 °C / Inert atmosphere

5.1: 24 h / 110 °C / Inert atmosphere

6.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C

With pyrrolidine; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 3.2: Wittig reaction / 5.1: Diels-Alder reaction;
DOI:10.1016/j.tet.2011.05.092

Reference yield:

: 1318051-97-6
C₂₁H₃₄O₂

: 1318052-37-7
C₃₂H₄₆O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 6 h / 0 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -60 °C / Inert atmosphere

2.2: 0.17 h / -60 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C

4.1: pyrrolidine / diethyl ether / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / 0 °C / Inert atmosphere

5.2: 8 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere

6.2: 0 - 35 °C / Inert atmosphere

7.1: 24 h / 110 °C / Inert atmosphere

8.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C

With pyrrolidine; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation / 5.2: Wittig reaction / 7.1: Diels-Alder reaction;
DOI:10.1016/j.tet.2011.05.092