dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

Base Information

Chemical Name:dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)
CAS No.:1097721-79-3
Molecular Formula:C₃₂H₃₇NO₆
Molecular Weight:531.649
Hs Code.:

Synonyms:dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

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Chemical Property of dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

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Technology Process of dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

There total 5 articles about dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 717879-45-3
dimethyl 6,6'-azanediylbis(3-tert-butylbenzoate)

: 610-97-9
o-iodo-methyl-benzoic acid

: 1097721-79-3
dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

Guidance literature:: With copper(l) iodide; copper; potassium carbonate; In diphenylether; at 190 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol801238n

Reference yield: 75.0%

: 610-97-9
o-iodo-methyl-benzoic acid

: 6,6'-azanediylbis(3-tert-butylbenzoate)

: 1097721-79-3
dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

Guidance literature:: With copper(l) iodide; copper; potassium carbonate; In diphenylether; at 190 ℃; for 48h; Inert atmosphere;
DOI:10.1002/chem.201706104

Reference yield:

: 34069-89-1
methyl 2‐[2‐(methoxycarbonyl)phenylamino]benzoate

: 1097721-79-3
dimethyl 6,6'-(2-(methoxycarbonyl)phenylazanediyl)bis(3-tert-butylbenzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / 2 h / 50 °C / Inert atmosphere

2: copper(l) iodide; copper; potassium carbonate / diphenylether / 48 h / 190 °C / Inert atmosphere

With aluminum (III) chloride; copper(l) iodide; copper; potassium carbonate; In diphenylether;
DOI:10.1039/c2jm32840b